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  • High density ablative thermal protection systems for reusable launch vehicles: processing, properties and thermal response evaluation

    Paper number

    IAC-11,C2,9,3,x11972

    Author

    Dr. Dona Mathew, Indian Space Research Organization (ISRO), India

    Coauthor

    Dr. Rajeev RS, Vikram Sarabhai Space Centre (VSSC), India

    Coauthor

    Mr. Deependran B, Indian Space Research Organization (ISRO), India

    Coauthor

    Mr. George Joseph, Vikram Sarabhai Space Centre, Thiruvananthapuram-695 022, INDIA, India

    Coauthor

    Dr. C. P. Reghunadhan Nair, Indian Space Research Organization (ISRO), India

    Year

    2011

    Abstract
    The aero heating encountered by reusable launch vehicles (RLV) warrants the use of a hot structures capable of withstanding the high temperature at the wing leading edge. Randomly oriented chopped silica fiber –phenolic resin ablative composites with varying fiber-resin compositions (70-90\% by weight) were developed for this application. The density of the composites varied from 1.3-1.6g/cc depending on the fiber-resin ratio. Compositional dependency of the composites on their mechanical and thermo-physical properties was examined. As the silica fiber content increased, the density and mechanical properties decreased due to poor wetting of the fibers and compaction. Thus, compared to the composition with 70\% fiber content, the tensile, compressive and flexural strengths reduced to nearly 50\% at a fiber loading of 90\%.  Coefficient of thermal expansion, thermal conductivity and thermal diffusivity of the composites exhibited a decreasing trend with increasing silica fiber content whereas, specific heat capacity increased as expected. Thermal simulations were carried out to evaluate the performance of the materials for the simulated heat flux history at the wing leading edge. The peak heat fluxes simulated for RLV re-entering at an attitude of 70 km were 90 W/cm2 during ascent phase and 35 W/cm2 during descent phase.  The thermal response was measured and the material surface behavior, mass-loss and flammability were studied. The mass-loss and back wall temperatures increased with increasing resin fraction in the composite. Ablation performance of the composites with higher silica content was superior, with diminished propensity for burning and formation of strong and intact char during kinetic heat simulation (KHS) tests. The mass-losses for compositions containing 80-90% silica fiber are less than 4\% by weight and the backwall temperatures are in the range of 250-290 °C.  Simulated thermal response of the composites was compared with that of an ideal system with zero mass-loss. The system with 90% silica fiber loading exhibited closest pattern to that of the ideal system. This was further corroborated by  KHS tests.
    Abstract document

    IAC-11,C2,9,3,x11972.brief.pdf

    Manuscript document

    (absent)