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  • The DLR Sample Analysis Laboratory - combining in-situ, remote sensing and sample analysis

    Paper number

    IAC-20,A3,4B,10,x55447

    Author

    Dr. Joern Helbert, Germany, DLR (German Aerospace Center)

    Year

    2020

    Abstract
    Building on the available infrastructure and the long heritage in spectral studies of planetary (analog) materials DLR is creating a Sample Analysis Laboratory (SAL). The setup has started with the installation of a vis-IR-microscope at the Planetary Spectroscopy Laboratory (PSL) in 2018. 
    
    Global reconnaissance of planetary surface can only be obtained by remote sensing methods. Optical spectroscopy from UV to far-infrared is playing a key role to determine surface mineralogy, texture, weathering processes, volatile abundances etc. It is a very versatile technique, which will continue to be of importance for many years to come. Providing ground truth by in-situ measurements and ultimately sample return can significantly enhanced the scientific return of the global remote sensing data. This motivates the planned extension of PSL with a SAL by support of the Astrobiology Laboratories.
    
    SAL will focus on spectroscopy on the microscopic scale and geochemical and geo-microbiological analysis methods to study elemental composition and iso-topic ratios in addition to mineralogy to derive information on the formation and evolution of planetary surfaces, search for traces of organic materials or even traces of extinct or extant life and inclusions of water.
    
    The current PSL and Raman facilities are operating in climate-controlled rooms and follow well-established cleanliness standards. The SAL will be housed in two ISO 5 clean rooms. The cleanrooms are equipped with glove boxes to handle and prepare samples. All samples will be stored under dry nitrogen and can be transported between the instruments in dry nitrogen filled containers.
    
    To characterize and analysis the returned samples the existing analytical capabilities are currently been extended. PSL was just upgraded with a vis-IR-microscope to extend spectral analysis to the sub-micron scale. 
    
    For the SAL this will be complemented by the following capabilities:
    1.	Electron Microprobe Analyse (EMPA) 
    for elemental analysis
    2.	Laser ablated inductive coupled Plasma Mass Spectrometer for elemental and isotope analysis
    3.	Dual Source TXRF & Grazing Incidence ED-XRF for mineralogical and structural analysis
    4.	Supporting equipment incl. microtome to prepare thin sections, optical polarization microscope, etc.
    
    Based on current planning the first parts of SAL will be operational and ready for certification by end of 2021. Analysis of first Hayabusa 2 samples can start by beginning to mid of 2022. 
    
    Following the approach of a distributed European sample analysis and curation facility as discussed in the preliminary recommendations of EuroCares (http://www.euro-cares.eu/) the facility at DLR could be expanded to a curation facility.
    Abstract document

    IAC-20,A3,4B,10,x55447.brief.pdf

    Manuscript document

    (absent)